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The NEXAFS spectra of the neat epoxy and the B-C-O monomers were also recorded to understand their contrast to the NEXAFS spectra of the B-C-O monomers in the BDM-B-GO nanocomposites. The NEXAFS spectra of the neat epoxy shows that the aromatic C-C and C-O-C bonds have disappeared and the C-C bond in the epoxy has shifted to 280.5 eV.
High frequency NEXAFS spectra at the carbon K-edge (Fig. 2) indicated the presence of five carbon environments. The first peak observed at 284.0 eV is attributed to the C-O-C bonds in the oxygenated groups. The next peak at 285.7 eV is ascribed to the C-C stretching of aromatic carbon species. The peaks observed at 286.6 and 287.5 eV are due to the C-O and C-C bonds in carboxylic and phenolic groups, respectively. The peak at 287.9 eV is due to the C-C bond in carbonyl groups. The third peak observed at 288.5 eV is due to the C-O-C bond in ether groups. The fourth peak observed at 289.9 eV is due to the C=O stretching in the ester groups.
The images show that there are no significant differences between the smooth surfaces of pristine GO, BDM-B-GO and MDA-B-GO. The small wrinkles on the surface of the 5% BDM-B-GO nanocomposite is attributed to the significant decrease of the surface energy of the sample. However, the surface roughness of the 5% MDA-B-GO nanocomposite is slightly higher than that of the 5% BDM-B-GO nanocomposite, indicating that the hydrophilic nature of MDA has not been completely reduced by BDM and the good compatibility between the two. Such an advantage is expected to increase the thermal stability of the thermoset.
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